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COR²E Facility Open House & Vendor Show

Monday, October 2, 2023, 11am to 1pm

Nuclear Magnetic Resonance Spectroscopy

Nuclear Magnetic Resonance Spectroscopy

Nuclear Magnetic Resonance Spectroscopy (NMR) determines the physical and chemical properties of atoms or the molecules in which they are contained and can provide detailed information about the structure, dynamics, reaction state, and chemical environment of molecules.

Contacts

General Contact

imsinfo@uconn.edu

Staff

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Nicholas Eddy, Ph.D.

Research Associate and Lab Manager
Nicholas.eddy@uconn.edu
860.486.2568

Location

Campus Address

Institute of Materials Science
Storrs Campus

Mailing Address

97 North Eagleville Road
Storrs CT 06269-3136

Instrumentation

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Bruker DMX 500 MHz High Resolution NMR Spectrometer

The Bruker DMX 500 MHz NMR spectrometer is a three-channel system dedicated for liquid samples with pulse field gradients capabilities. The spectrometer is equipped with a 5 mm inverse triple resonance gradient probe with a three axes XYZ Great 3/10 gradient amplifier and a 5 mm double resonance multinuclear broadband probe with a BVT-2000 Eurotherm VT Control Unit.

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Bruker DMX 300 MHz Solid-State NMR Spectrometer

The Bruker DMX 300 MHz Wide Bore (WB) NMR spectrometer is a two-channel system dedicated for solid samples with Magic Angle Spinning (MAS) capabilities. The spectrometer is equipped with a double resonance 7 mm MAS probe and a double resonance 4 mm MAS probe for solids with VT from – 50 to +150 degrees Celsius running experiments with Nitrogen gas. This instrument also has a double resonance 5 mm multinuclear broadband probe for liquid samples.

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Bruker Avance III 400 MHz Solid-State NMR Spectrometer

The Bruker Avance III 400 MHz Wide Bore (WB) NMR spectrometer is a three-channel state-of-the-art system dedicated for solid samples with Magic Angle Spinning (MAS) and Pulse Field Gradient capabilities. The spectrometer is equipped with a triple resonance HXY 4 mm MAS probe and a triple resonance HFX 2.5 mm MAS probe for solids with VT from – 50 to +150 degrees Celsius running experiments with Nitrogen gas. This instrument also has a double resonance H(F)X 5 mm Doty Scientific Pulse Field Gradient (PFG) probe with a Z axis Great 1/40 gradient amplifier for diffusion studies of liquid and solid samples.